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Ice and Pore Structure Investigations on the Micro-scale

Since polar ice cores are used as climate archives it is worthwhile to understand the processes that form and change the archive during time. Polar snow and firn layers build up with time and do change their properties while they become buried and transformed to ice. The characteristics of the surface snow layers are preserved in the resulting ice. Important conclusions about such processes can be drawn from measurements of the physical properties with depth starting with investigations of the pore and ice structures at the snow-atmosphere interface down to the firn-ice transition where atmospheric air is enclosed into the ice (polar ice as the only gas-archive on earth).


 

Further down the micro-structures are recorded in order to investigate the dynamical behaviour of ice caps and track micro-inclusions. As ice is a highly anisotropic material due to its hexagonal crystal system, various processes on atomic scale (e.g. dislocation climb and glide, diffusional processes etc.) are always competing in deformation and keep the question on the dynamical behaviour alive in research. These processes are acting on the atomic scale and are therefore difficult to observe directly in deforming polycrystalline samples. However, they leave behind certain structures on the microscopic scale indicating deformation mechanisms. The single mechanisms, such as grain rotation or grain boundary sliding, can be observed by the study of c-axes evolution, grain size evolution and other microstructural observations. The processes, which should be dominant along the creep history of polycrystalline ice should be known to interpret the deformation history of an ice core.


 

Experimental methods
The µCT measurements are performed with the means of two portable CT-Scanners (Skyscann CT1074 and CT1072) operating at around -15°C in a cold lab (or field lab). The resolution varies between 40 µm (CT1074) and 8-20 µm (CT1072). The sample size is restricted to cylinders with a diameter of 30 mm (CT1074) and 20 mm (CT1072). The three dimensional reconstructions are analyzed with a series of image tools for volume images (MAVI, ImagePro, NIH-Image) and parameters like open and closed porosity, surface density, pore and ice intercept length, grain and pore size distributions, Euler number, coordination number, geometrical tortuosities and other three dimensional shape factors are estimated.


 

The micro-structure mapping system (µSM) records features with about 3 µm resolution on planes of 100x100 mm that are visible by an optical microscope in reflected and transmitted light. Important detected features are grain boundaries, sub-grain boundaries, slip bands, micro-inclusions, micro bubbles and air clathrates (Fig µSM).
The optical linescanner records features with a much lower resolution of only 100 µm in transmitted light. The features are continuously measured on 10 mm thick sections of up to 100 cm length and 10 cm width. The grey value images are mainly used to visualize the stratigraphy and potential disturbances of the layering along the whole ice core.
The fabric analyzer measures crystal orientation fabrics and textural parameters such as crystal size, crystal elongation. In addition, by image processing techniques the individual crystals are recognized automatically and other parameters, such as grain size and grain shape, can be estimated simultaneously.


 

Models
3D-percolation model on a BCC-lattice for the simulation of pore closeoff
Lattice Boltzmann Models for diffusion and advection in 3D-pore structures to derive the effective diffusivity (tortuosity) and permeability on the small scale pore space.


 

Running Projects:

  • Improvements of image processing tools for µCT of snow and ice (Freitag, Hoerhold)
  • In-Situ µCT of Antarctic snow, 3D-pore reconstructions of polar firn and ice (Freitag, Hoerhold)
  • The fate of snow dunes at Kohnen Station, Dronning Maud Land, Antarctica (Freitag, Kipfstuhl)
  • Development of an improved dating tool for gas enclosures in stratified firn (Freitag, Kipfstuhl)
  • Investigations of the climatic impact on polar Firn structure using µC-Tomography  (DFG funded Project INFITO), (Hoerhold, Freitag)
  • Micro-structure analysis of EPICA DML deep ice cores including textural parameters (grain size, grain shape, sub-grain boundary occurrence, slip line occurrences) and fabrics (c-axes distributions), (Weikusat, Kipfstuhl)
  • Investigation of sub-grain boundary formation processes in ice (Weikusat)
  • Evolution of ice crystal micro-structures during creep experiments (Weikusat, Kipfstuhl)

 
Participants
Dr. Sepp Kipfstuhl, Dr. Johannes Freitag, Dr. Ilka Weikusat


 
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